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Murat Kalemci, Sevilay Ugur
THE CONSTRUCTION AND CHARACTERIZATION OF PLATINUM-BASED THERMOCOUPLES AT UME

High accuracy measurement of temperature up to 1200°C is an important concept for science, technology and for the industry. For high temperature measurements, thermocouples, which depend on Seebeck principle, are widely used. Platinum based thermocouples are preferred due to their high purity and quality for metrological use. In this paper, the construction of type S and type R thermocouples at UME will be described. After construction, thermocouples were calibrated at the tin, zinc, aluminium and silver freezing points by fixed-point method and by wire-bridge method at gold point.

Marcelo dos Santos Monteiro, Alcir de Faro Orlando
STABILITY EVALUATION OF A GOLD-PLATINUM THERMOCOUPLE AS AN INTERPOLATING INSTRUMENT IN THE TEMPERATURE SCALE

The 1990 International Temperature Scale (ITS-90) substituted the platinum-platinum-10% rhodium thermocouple by the high temperature standard platinum resistance thermometer (HTSPRT) and the radiation thermometer, as an interpolating instrument in the 630°C to 1064°C range, due to the lower stability of the thermocouple. Although the uncertainty of reproducing the temperature scale became much lower, the cost of the required measuring equipments was raised. Aiming to offer the Brazilian Calibration Network accredited laboratories a lower cost temperature scale traceability alternative, at a smaller uncertainty than the standard type S thermocouple can provide, a 99,999% purity gold-platinum (AuPt) thermoucouple was exposed systematically to a high temperature environment (close to 1000°C) for more than 1500 hours, with its stability and homogeneity being evaluated with the aid of a silver fixed point cell. It was shown that a ± 25 mK (k=2) uncertainty can be achieved. This works details the methodology and the cares that have to be taken in order assure the reliability of the results.

Georges Bonnier, Eliane Renaot, DavorZvizdic, Lovorka G. Bermanec, Tomislav Veliki
MODEL FOR UNCERTAINTY ESTIMATION IN COMPARISON CALIBRATION OF THERMOCOUPLES

The objective of this paper is to present the methodology for estimation of measurement uncertainties in comparison calibration of thermocouples used at Laboratory for Process Measurements (LPM). The methodology is applied for comparison calibration of rare-metal and industrial basemetal thermocouples within temperature range from –20°C to 660°C with LPM standard/working standard platinum resistance thermometers and from 600°C to 1050°C with LPM standard/working standard thermocouples.

Frank Bernhard, Dirk Boguhn, Silke Augustin, Helge Mammen, Andrej Donin
APPLICATION OF SELF-CALIBRATING THERMOCOUPLES WITH MINIATURE FIXED-POINT CELLS IN A TEMPERATURE RANGE FROM 500°C TO 650°C IN STEAM GENERATORS

Using integrated miniature fixed-point cells, a measuring uncertainty of < 1 K can be reached under operating condi tions in the superheated steam range of power plants by a periodic recalibration of the thermocouples, with operating times of > 20000 h. The fixed-point materials used for a temperature range from 500°C to 650°C are technically pure metals and binary alloys.

Emese András
THE INFLUENCE OF SURFACE INCLINATION ON THE CALIBRATION OF SURFACE TEMPERATURE SENSORS

The OMH has developed a reference surface temperature apparatus for the calibration of contact surface temperature sensors under a variety of conditions. This article describes the dependence of temperature error on the inclination of a heated surface and studies the sources of these deviations for various surface temperatures and sensor types. The effect of surface inclination has not been investigated before but has been found significant, particularly because of its industrial relevance.

Rick Walker, Norman Willgress
ACHIEVING 0.25 mK UNCERTAINTY WITH AN INTEGRATED-CIRCUIT RESISTANCE THERMOMETER READOUT

Resistance bridges, when used for temperature measurements with SPRTs, are able to achieve uncertainties better than 1 ppm. However, they have several shortcomings that prohibit their use in many applications. Among these are cost, size, slow speed, and limited range. An endeavor was made by the author to design a readout for resistance thermometers that achieves less than 1 ppm uncertainty in resistance ratio while overcoming some of the problems of resistance bridges. A new approach was taken with a design that uses the latest integrated-circuit analog-todigital converters. This allows the instrument to have lower cost, smaller size, the capability of increased speed, and additional features. Special effort was made to reduce errors caused by component drift, thermoelectric EMF, component offset, electrical noise, and nonlinearity. The new resistance thermometer readout was tested to identify and evaluate sources of measurement uncertainty. The combined uncertainty was calculated for resistance ratio and W(T90) measurements of an SPRT with self-heating corrections. Measurements made with the resistance thermometer readout were compared with measurements made with a resistance bridge. The results show that the standard uncertainty of the new resistance thermometer readout is about 0.34·10-6 in measuring resistance ratio at 25 Ω/100 Ω and about 0.68·10-6 in measuring W(T90) near the triple point of water.

Ali Uytun, Aliye Kartal Dogan, Sevilay Ugur
CONSTRUCTION AND CHARACTERISATION OF THE UME MADE WATER TRIPLE POINT CELLS

The International Temperature Scale of 1990 (ITS-90) specifies triple, melting and freezing points to realize the scale. One of the major temperature fixed points in the ITS-90 scale is the triple point of water (TPW), at which temperature solid, liquid and vapour phases of pure water coexist in thermal equilibrium. This temperature has been assigned a value of 273,16 K (0,01°C) on the ITS-90. It is the fundamental definition of the fixed point of the ITS- 90 scale and the one defining fixed point of the Kelvin thermodynamic temperature scale.
UME Temperature Laboratory has been constructing TPW cells since 1992. This paper describes the construction processes (annealing, cleaning and filling) of the TPW cell, its realization and finally the results of EUROMET comparison of TPW cells.

John Redgrove
EUROPEAN VIRTUAL INSTITUTE FOR THERMAL METROLOGY

A European Virtual Institute for Thermal Metrology (EVITherM) is being developed by a consortium of 34 European institutes, led by NPL and supported by the EC, to ensure that thermal knowledge and services are made available to industry, for the benefit of industrial processes and the environment, offering low-cost easy access, particularly to SMEs. EVITherM will be a co-ordinated Internet-based infrastructure designed to link together the geographically scattered centres of excellence and other groups and organisations concerned with thermal measurements and technology to provide a focal point for information exchange and knowledge transfer between all these organisations and industry. It will form a website for users, having three levels of access. The first level is free and contains directories of information; the second and third levels are for members only and will allow access to qualified information and member interactions. The first public release of the website is due by early 2004.

Dražen Klaric, Bojan Mazanek, Mladen Boršic
FACING THE XVII IMEKO WORLD CONGRESS – HOW WE DID IT

IMEKO World Congress is gathering of experts in the field of metrology. More than 500 abstracts have been received during last year and even more people have registered for attending it. Huge number of applications required usage of modern technologies including Internet as a backbone for communication and interaction among participants and organisers. From one excel table we developed powerful web based application that can handle more than 5000 records thus enabling us to overcome difficulties that faced us during organisation of the congress.
In this paper we describe how Croatian Metrology Society dealt with the challenge of organising IMEKO World Congress. We discuss about technologies used to attain multi user environment and accessibility of data to entire organising committee. Something about security issues related to revision process of not yet published papers would be pointed out. We will illustrate some examples of our software for automate of the registration process.

Fiona Redgrave, Andy Henson, Diane Beauvais
METROLOGY FOR IMPROVED MEASUREMENTS IN INTERNATIONAL REGULATION AND TRADE: THE REGMET AND METROTRADE PROJECTS

The operation of the economy on a global scale and the quality of life for the individual citizen depends on reliable measurements and tests, which are trusted and accepted internationally. The European Commission is supporting two projects linking measurement, regulation, trade and commerce under the Competitive and Sustainable Growth thematic Programme in the Fifth Framework Programme. This paper describes the aims and some findings of the RegMet and MetroTrade projects, including the concept of the development of a measurement template for regulators.

Page 903 of 939 Results 9021 - 9030 of 9382