IMEKO Event Proceedings Search

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Gaber Begeš, Valentin Batagelj, Igor Pušnik
INFLUENCE OF A MEASUREMENT UNCERTAINTY OF A COLD JUNCTION IN TESTING OF HEATING

Testing of safety of electrical appliances is very important for assuring of safety of users. One of the safety tests is testing of heating of appliances and their surrounding. The test is performed in a measurement system so called "black test corner", which is partially standardised. Measurement of heating is performed with thermocouples. This paper describes the analysis of the influence of the measurement uncertainty of a cold junction of a thermocouple in testing of heating. Heating of appliances is measured as a difference between the temperature of the appliance and the temperature of the surrounding. If the cold junction of a thermocouple is exposed to temperature of the surrounding the thermocouples measure the heating and not the absolute temperature. The measurement uncertainty and the temperature value of the cold junction must be known for proper measurement and uncertainty evaluation.

Bojan Acko
EXPERIMENTAL ANALYSIS OF UNCERTAINTY OF SQUARENESS CALIBRATION ON A CO-ORDINATE MEASURING MACHINE

Co-ordinate measuring machines (CMMs) are often used for calibrating different kinds of squares. A procedure for calibrating squares on the CMM Zeiss UMC 850 was developed in our laboratory to cover primarily industrial needs. The uncertainty analysis that was performed for this procedure is introduced in the article. The most important uncertainty contributions were evaluated experimentally. Many experiments were also performed in order to find the most appropriate calibration position in the CMMs measurement space. About 2000 measurement points were taken in order to get reliable results for uncertainty components. The analysis results expressed as the best measurement capability were checked by participation in the Euromet 570 project, which has not been finished yet. The current value of the best measurement capability is 0,9 arc sec.

M.Teresa López, M.Belén. Martín, M.Teresa Doria, Susana Rodriguez
EVALUATION OF MEASUREMENT STANDARDS

Centro Español de Metrología (CEM), Spanish Metrological Institute, as part of its activity, has started to prepare primary reference gas mixtures using gravimetrical method. As a consequence of this new work, a comparison of some primary reference gas mixtures prepared by CEM has been carried out with three of the gas mixtures manufacturers established in Spain. CEM has coordinated this comparison with the manufacturers in order to assure traceability in equipments for the automotive exhaust gas field. The objetive of this comparison is double:
• to compare the analytical results with the gravimetric value of Primary Standard Material (PSM) preparation,
• to compare the measurement capabilities between laboratories in measuring the amount of substance fractions of carbon dioxide in nitrogen.

Hiroshi Sato, Kensei Ehara
DETERMINATION OF UNCERTAINTY ASSOCIATED WITH QUANTIZATION ERRORS USING THE BAYESIAN APPROACH

In practice, quantization of a measured quantity often significantly influences observation values. A typical example is found in measurements using digital instruments. In some cases, due to the quantization, no dispersion is observed among repeated measurements. The type A evaluation then gives zero standard uncertainty. In such a case, the most common practice is to assume, as an a priori distribution in type B evaluation, a uniform distribution, the width of which is given by the quantization interval, and take the width divided by square root of 12 as the standard uncertainty.
This practice, however, is justified only when the population standard deviation is exactly zero. But generally this condition does not hold true even if the sample standard deviation appears to be zero. In the present study, we use the Bayesian approach to evaluate the uncertainty of a measurement based on quantized data with due consideration to the difference between the standard deviation of the apparent sample and the population standard deviation.
We assume that the quantity before quantization obeys a normal distribution having the average µ and standard deviation σ. A measurement data corresponds to a value of the quantity after quantization. Based on a specific combination of n repeated measurements, we can construct the probability density p(µ, σ) using the Bayesian method. The standard deviation of the function, p~(µ) = ∫p(µ, σ)dσ , in terms of µ gives the uncertainty of the measurement result. We have shown that when all of the measurement data take the same value, the conventional type B evaluation described the above results in an underestimate of the uncertainty, if the number of data is less than five. Analysis is also conducted in cases in which not all of the data take the same value.

Yasuo Iwaki, Tadao Inamura, Komyo Kariya
DATA MINING OF UNCERTAINTY DATA IN THE BLOOD CHEMICAL ANALYSIS FOR QC

This study is mining the error factors in the uncertainty measurement data. The purpose is to be advanced the accuracy control for QC (Quality control) of BCA (Blood Chemical Analysis). BCA is often taken as uncertainty data. On the QC of calibration curve, it is important to securing an intermediate accuracy in the measuring system of ISO-GUM (International Organization for Standardization-Guide to the express of Uncertainty Measurement). In the technology of ISO-GUM, the analysis method of traceability, transferability and compatibility are applied. Already we have reported the uncertainty problems as series of three times in the IMEKO world congress.
1) 1997.in Finland. The reference value was chosen by transferability of ISO-GUM.
2) 1999.in Japan. The error factor was taken in time series data by traceability of ISO-GUM.
3) 2000.in Austria. The Michaels-Menten test should be practiced by using the compatibility of ISO-GUM.
These reports were studied by using only one of test reagent of Elastase-1, which is a kind of human pancreas hormone. The study has been continuing by using other 4 kinds similar sample. Then the purpose of this study is an experiment to get more high reliability. In this thesis, a new result on uncertainty problem is reported.

Adriana Horníková
ANALYSIS OF MEASUREMENT OF INTER-LABORATORY COMPARISON THROUGH CONFIDENCE INTERVALS (No 46)

It is possible to compute uncertainty in the form of confidence intervals. In this article is exploited the confidence intervals determination through a simulation study that enables to evaluate uncertainty in the form of confidence intervals for real measurements of inter-laboratory comparison (ILC) even for small numbers of observations.
Here are listed estimation approaches (mathematical-statistical algorithms) for the determination of the consensus value (the true measured value); confidence interval for the true measured quantity in different laboratories; determination (estimate) of the inter-laboratory variance; confidence interval for the inter-laboratory variance; and within-laboratory variance in experiment of the inter- laboratory comparison with homoscedastic as well as heteroscedastic measurements. Different possibilities of evaluation of ILC when the model applied is a linear model with one random effect "laboratory" and estimation procedures are listed and discussed (also describing of the statistical features) in this contribution.
The merit of the simulation study is for a statistician (evaluator of ILC) in better approximation of needed confidence level to obtain the expected result precision in balanced and unbalanced experiment design for homoscedastic as well as heteroscedastic measurements when having small number of observations.

Siva Venkatachalam, Jay Raja
AN INTERNET BASED GAGE R&R AND UNCERTAINTY ANALYSIS SYSTEM

In a world where the gap between the macro and the micro scales is on the increase, measurement and measurement procedures assume significant importance. In an effort to produce high quality products, industries employ state-of-the-art manufacturing techniques. The best manufacturing techniques would be meaningless without being complimented by the best measurement system and procedures in order to get accurate measurement results. The present industrial scenario is such that the measurement process has become increasingly tedious and also subject to a lot of constraints.
Traceability (VIM 6.10), a requirement for quality standard certification, is the property of the result of a measurement or the value of a standard whereby it can be related to stated references, usually national or international standards, through an unbroken chain of comparisons all having stated uncertainties. In order to establish traceability, measurement results must be accompanied by a statement of uncertainty. The theory and computation of measurement uncertainty requires a certain degree of knowledge and expertise and so in most cases, the industry follows a much simpler procedure called gage repeatability and reproducibility (Gage R&R) to represent the total variation in the measurement system. The need for simple tools for estimation of Gage R&R and measurement uncertainty has provided the motivation for us to build an internet based software system for the estimation of Gage R&R and measurement uncertainty.

Alexander I. Zaiko, Natalia A. Zaiko
ACCURACY OF STATISTIC AND SPECTRAL MEASUREMENTS

The paper is concerned with attempts to investigate the influence of measurement results errors, the algorithms for signal values recovering between the measurement actions, time discrete period, the samples number, and the interval of signal observation as well as other factors on the procedures of statistic treatment of measurements results. The application of the obtained procedures for measurement precision assessment to knowledge base creation provides a possibility to increase the intelligent measurement efficiency.

Giovanni B. Rossi, Francesco Crenna, Michele Codda
COMPUTER AIDED EVALUATION OF MEASUREMENT UNCERTAINTY BY CONVOLUTION OF PROBABILITY DISTRIBUTIONS

The evaluation of measurement uncertainty, from the final user’s standpoint, involves several issues which are only partially addressed by the GUM. An evaluation procedure assisted by a computer program can be of great support and provide the user with detailed results useful for further analysis. In this paper a code is presented for the assisted evaluation of measurement uncertainty, based upon the convolution of probability distributions. So the method allows expression of the final result of measurement as a probability distribution, on which it is possible to evaluate useful parameters such as expanded uncertainty, at whatever confidence level. It also permits to evaluate, in probabilistic terms, the risk associated to matching tolerances. Moreover it is possible to manage the uncertainty on dispersion parameters (sometimes called ‘uncertainty of uncertainty’) considering a modified probability distribution. In the paper the code is presented together with some case studies showing the support available to the operator, the GUM compatibility and the application importance of the final probability distribution.

Tanasko Tasic, Roman Flegar
VALIDATION OF CUSTOM DEVELOPED SOFTWARE IN METROLOGY APPLICATIONS

Requirements for validation of custom developed software in metrology applications are mainly influenced by technical realisation of measuring instrument/system. In this article some issues related to the technical realisation of validated software are described. Furthermore, the state-of the art validation approaches and tools are presented, including failure risk analysis and test case selection. In the discussed example the validation approach in case of MIRS Mass Laboratory automation software is presented. Synthesis of presented methods, tools and techniques may be useful as guidance for validation of similar software applications.

Page 910 of 939 Results 9091 - 9100 of 9382