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Andreas Brüge
CREEP MEASUREMENT IN REFERENCE TORQUE CALIBRATION MACHINES

Creep measurements in reference torque calibration machines cannot be performed like those in direct load calibration machines. Comparisons between creep measurements in both situations lead to recommendations for reference methods yielding results which are equivalent to results based on direct load methods. Furthermore, some effects are discussed which might affect the comparability of creep measurements.

Christian Diethold, Thomas Fröhlich, Falko Hilbrunner, Gerd Jäger
HIGH PRECISSION OPTICAL POSITION SENSOR FOR ELECTROMAGNETIC FORCE COMPENSATED BALANCES

This paper discusses an optical position sensor which can be used in balances based on the principle of electromagnetic force compensation (short used EFC) for example. Other applications are zero point detection as well as high precision positioning in the range of ± 200 μm. The position sensor consists of two infrared-LED (IR-LED) which illuminate a single photodiode via an aperture. The aperture is movable and performs a shadowing of the beams, thus shadowing changes due to the position of the aperture. The photodiode detects light from both LED. Both light sources have to be modulated and phase shifted to distinguish them in the photodiode signal. The evaluation of the position of the aperture is done by demodulating the received signal.
A major advantage of this method is that the aperture's operating point is in the centre of the beams. Hence higher sensitivity is achievable and the beams can be focused onto the photodiode. Furthermore standard components are used and thus expensive differential photodiodes are no longer necessary.

Goutam Mandal, C. K. Gopan
IMPROVEMENT OF MEASUREMENT CAPABILITIES OF MULTIPLE MASS STANDARDS OF 1 kg AT NPLI

The National Physical Laboratory, India (NPLI) is the custodian of National Prototype of the Kilogram (NPK) No. 57, which was provided by the International Bureau of Weights and Measures (BIPM), Paris, France in 1958 after its first calibration in 1955. The NPK has been recalibrated three times (1985, 1992 & 2002) so far at the BIPM. All NPL working standards (Multiples & sub-multiples of 1 kg) range from 1 mg to 20 kg are reestablished using new value of NPK through four Transfer Standards of 1 kg (two made of Stainless steel and two made of Nickel-Chromium alloy) according to defined periodicity.
The calibration of multiples of 1 kg is carried out using a fully automatic mass comparator with maximum capacity of 64 kg and resolution of 0.1 mg. Using this mass comparator, we have improved our calibration and measurement capabilities (CMCs) from 0.6 mg to 0.2 mg (k = 2) in 2 kg, from 1.5 mg to 0.3 mg (k = 2) in 5 kg, from 3 mg to 0.5 mg (k = 2) in 10 kg and from 6 mg to 1.0 mg (k = 2) in 20 kg. The details of measurement technique and results of multiples of 1 kg are discussed in this paper.

Wirun Laopornpichayanuwat, Jakkapol Visessamit, Montian Tianprateep
3-D SURFACE ROUGHNESS PROFILE OF 316-STAINLESS STEEL USING VERTICAL SCANNING INTERFEROMETRY WITH A SUPERLUMINESCENT DIODE

Surface roughness is one of many parameters that influences on mass stability of standard weight, commonly used as a transfer standard of mass SI unit. One of the most famous non-invasive methods for determining surface roughness from a surface profile of material is a vertical scanning interferometry (VSI) with a white light source. In this research, 3-D surface profiles of 316-stainless steel, usually used as a material for standard weights, are constructed by using VSI, based on Michelson interferometer (MI). Because of its low-coherent properties, low cost, and compact light source, a superluminescent diode (SLD) is chosen as a low-coherence light source in our interferometry system. Since a continuous wavelet transform (CWT) algorithm provides accuracy results, it is also used as a numerical analyzing method for the interferogram signals, taking from our VSI. The surface roughness and measurement uncertainty, calculated from the constructed 3-D surface roughness profiles of 316-stainless steel samples, are discussed.

Thomas Fröhlich, Thomas Fehling, Detlef Heydenbluth, Matthias Geyer, Ralf Schüler
VACUUM TRANSFER SYSTEM FOR LOADING THE SARTORIUS PROTOTYPE MASS COMPARATOR CCL1007

The Vacuum Transfer System (VTS) is designed for fully automatic loading of weights into the Sartorius Prototype Mass Comparator CCL1007. The system enables the user to transfer weights from air to air/neutral gas, air to vacuum and back, as well as from vacuum to vacuum conditions. A detailed description of the technical parameters and the different operation modes will be presented.

Dominik Pražak, Jaroslav Zůda, Ladislav Peksa
CALIBRATION OF SECONDARY STANDARD LEAKS BY MEANS OF MASS COMPARISON

Gas leak detection is getting more important in the last years. Primary standards for leaks can be divided into sensitive and insensitive to gas species. The method proposed by authors is insensitive to gas species. The basic principle of the method is mass comparison and detection of the difference between standard weight and the leak to be calibrated. The authors made several measurements to prove the repeatibility of the method. It can be seen that to get results with reasonable uncertainty the weekend measurement is sufficient.

Stuart Davidson, Michael Perkin
AN INVESTIGATION OF DENSITY DETERMINATION METHODS FOR POROUS MATERIALS, SMALL SAMPLES AND PARTICULATES

Three new density measurement techniques have been devised and evaluated for the measurement of nonstandard objects, namely porous material samples, small solid samples, powders and particulates. Hydrostatic weighing has traditionally been used to determine the density of solid artefacts. This method is not, however, suitable for porous objects since they will adsorb water making weighing in water unstable and possibly detrimental to the material samples. A method, weighing the artefacts in inert gas, has been developed for this application. The density determination of small solid artefacts cannot be achieved by conventional hydrostatic weighing techniques due to limits on the accuracy with which the weight-in-water can be determined A density gradient column method for such measurements, delivering very low uncertainties, has been developed and evaluated. A liquid pyknometry method has also been investigated as an alternative to traditional helium and mercury pyknometry. The technique offers improved accuracy and a precise determination of thermal coefficient of the sample under test.

F. Hilbrunner, H. Weis, T. Fröhlich, G. Jäger
COMPARISON OF DIFFERENT LOAD CHANGERS FOR EMFC-BALANCES

In order to further improve the metrological properties of weighing systems based on the principle of electromagnetic force compensation (EMFC) as well as quality assurance, it is necessary to determine the parameters relevant for the dynamic operation, such as measurement time and controller behavior. This determination is carried out by loading the balance system and observing the indication. Typically this is done by a load changer using different metrological weights. This method is inevitable if metrological traceability is required. However, the conventional procedure of load changing also entails several disadvantages. The number of possible load changes per unit time is limited and the force characteristic during loading is usually unknown and relatively difficult to reproduce or manipulate. Furthermore the fast and sudden exchange of the weights causes mechanical vibrations and a movement of the surrounding air, both of which act as additional disturbances.
In this paper we propose an alternative loading method, with which these shortcomings can be improved and compare it to a conventional system. This method is based on loading the weighing system in a defined manner using a Lorentz-force, allowing the tester to generate a known, virtually arbitrary force characteristic during loading.
It is shown that the Lorentz-force generated load represents a practical alternative to classical weights, offering advantages in reproducibility, dynamics and ability to be automated. Since the proposed method applies a known Lorentz-force to the weighing system it becomes possible to exactly determine the relationship between the force acting on the weighing pan and the resulting behavior of the weighing system.

David Gichangi Axelson, Koji Tada, Tuan Le, Shinichi Hayashida, Toshio Uchimaru, Yutaka Yamamoto
DYNAMIC AXIS SCALE WITH HIGH ACCURACY FOR HIGH SPEED MEASUREMENT OF VEHICLE MASS

As the demand for measuring objects in motion is increasing the need for a system to measure vehicles has been developed to measure mass of vehicle in dynamic motion. Using the concept of measuring the inertial mass of a moving vehicle instead of gravitational mass has proven successful for a purely dynamic problem.
Since the measurement of a dynamic motion requires high speed sampling a scanning speed of the signal information is set at 1μs/sample. This is to ensure the movement of the structure is captured to full extent.
Using dynamics, the inertial mass correlation between the Dynamic Axis Scale and the vehicle can be calculated from the dynamic state of the vehicle in motion. The achieved result is instantaneous and currently reliable from 0 km/h up to 80 km/h with an high accuracy with ± 5% of error tolerance of the measured mass provided the vehicle mass is restricted to EU regulation for public roads of 20 ton. Measuring the momentum of the vehicle and calculating the speed to the relation of mass, it can verify the dynamic calculation and thus confirm the inertial mass of the vehicle.

Nieves Medina, José Ángel Robles
NON AUTOMATIC WEIGHBRIDGES SCALES INTERCOMPARISON IN SPAIN: A DIFFERENT APPROACH

This paper shows an interesting case for a national comparison where two transfer standards have been used. Participating laboratories have calibrated one transfer standard or the other, but one that calibrated both, so that can be used as a link to make a joint evalution for all the participant laboratories.

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